Transition metal analysis: A comparison between ICP-AES and deuteron activation

A. E. Pillay, J. R. Williams, M. O. El Mardi, S. M. Hassan, A. Al-Hamdi

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Abstract

The analytical capabilities of ICP-AES (ICP) and deuteron activation (associated with prompt gamma-rays and delayed X-rays) for the determination of certain transition metals, were investigated. The sensitivities of the three methods are given, and the general applicability of each technique is evaluated. In the case of ICP, numerical data were obtained from aqueous solutions containing digested plant material. These experimental results were assessed against minimum detectable limits attained in relevant solid matrices that were subjected to prompt gamma-ray and delayed X-ray spectrometry using 5 MeV 2H+ ions. The analytically useful lines originated mainly from (d,p) and (d,n) reactions. The potential of the three techniques for routine analysis is discussed and detailed methodologies are presented.

Original languageEnglish
Pages (from-to)465-467
Number of pages3
JournalJournal of Radioanalytical and Nuclear Chemistry
Volume254
Issue number3
DOIs
Publication statusPublished - Dec 1 2002

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ASJC Scopus subject areas

  • Analytical Chemistry
  • Inorganic Chemistry
  • Nuclear Energy and Engineering

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