Application of low dose techniques to structure determination in a transition metal-containing poly-yne

A. E. Dray; A. M. Donald; R. H. Friend; M. S. Khan; J. Lewis; R. Rachel; W. O. Saxton

Application of low dose techniques to structure determination in a transition metal-containing poly-yne

A. E. Dray^*, A. M. Donald, R. H. Friend, M. S. Khan, J. Lewis, R. Rachel, W. O. Saxton

^*Corresponding author for this work

Chemistry

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution

Abstract

Organometallic polymers have potential applications in opto-electronics but full understanding and utilisation of their properties requires knowledge of the polymer structure and possible structural defects. In this work we present a summary of results obtained using high resolution electron microscopy (HREM) and a variety of low dose techniques in order to obtain lattice images of a well crystallised, beam sensitive Pt-containing poly-yne. Many details of the unit cell and of typical lattice defects have been obtained via HREM on a polymer system for which single crystal x-ray diffractometry has proved impossible.

Original language	English
Title of host publication	Institute of Physics Conference Series
Publisher	Publ by IOP Publishing Ltd
Pages	349-352
Number of pages	4
Volume	119
ISBN (Print)	0854984089
Publication status	Published - 1991
Event	Proceedings of the Institute of Physics Electron Microscopy and Analysis Group Conference - Bristol, Engl Duration: Sep 10 1991 → Sep 13 1991

Other

Other	Proceedings of the Institute of Physics Electron Microscopy and Analysis Group Conference
City	Bristol, Engl
Period	9/10/91 → 9/13/91

ASJC Scopus subject areas

Physics and Astronomy(all)

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Application of low dose techniques to structure determination in a transition metal-containing poly-yne. / Dray, A. E.; Donald, A. M.; Friend, R. H.; Khan, M. S.; Lewis, J.; Rachel, R.; Saxton, W. O.

Institute of Physics Conference Series. Vol. 119 Publ by IOP Publishing Ltd, 1991. p. 349-352.

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution

Dray, AE, Donald, AM, Friend, RH, Khan, MS, Lewis, J, Rachel, R & Saxton, WO 1991, Application of low dose techniques to structure determination in a transition metal-containing poly-yne. in Institute of Physics Conference Series. vol. 119, Publ by IOP Publishing Ltd, pp. 349-352, Proceedings of the Institute of Physics Electron Microscopy and Analysis Group Conference, Bristol, Engl, 9/10/91.

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AU - Lewis, J.

AU - Rachel, R.

AU - Saxton, W. O.

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AB - Organometallic polymers have potential applications in opto-electronics but full understanding and utilisation of their properties requires knowledge of the polymer structure and possible structural defects. In this work we present a summary of results obtained using high resolution electron microscopy (HREM) and a variety of low dose techniques in order to obtain lattice images of a well crystallised, beam sensitive Pt-containing poly-yne. Many details of the unit cell and of typical lattice defects have been obtained via HREM on a polymer system for which single crystal x-ray diffractometry has proved impossible.

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