ملخص
An automated method for the determination of trimeprazine and perphenazine by complexation with palladium(II) in hydrochloric acid was developed. A sequential injection technique with a flow reversal of 29.4 s-1 and a measuring cycle of 73 s was used. Trimeprazine in the range 50-400 ppm was determined at pH 4.7 using 5.0 × 10-3 moll-1 palladium(II) solution and monitoring the product spectrophotometrically at 515 nm. Perphenazine in the range 50-500 ppm was determined at pH 4.85 using 2.5 × 10-3 mol l-1 palladium(II) solution and monitoring the product at 560 nm. The technique was successfully applied to the determination of reaction stoic-biometry. Interferences were studied and the method was found to be suitable for the determination of the two compounds in pharmaceutical preparations.
اللغة الأصلية | English |
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الصفحات (من إلى) | 561-563 |
عدد الصفحات | 3 |
دورية | The Analyst |
مستوى الصوت | 120 |
رقم الإصدار | 2 |
المعرِّفات الرقمية للأشياء | |
حالة النشر | Published - 1995 |
منشور خارجيًا | نعم |
ASJC Scopus subject areas
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